3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

Base Information

Chemical Name:3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one
CAS No.:94448-08-5
Molecular Formula:C₂₁H₂₃N₃O₃
Molecular Weight:365.432
Hs Code.:

Synonyms:3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

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Chemical Property of 3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

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Technology Process of 3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

There total 5 articles about 3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 94447-95-7
3-(2-aminoanilino)-4,4-dimethyl-2-buten-4-lactam

: 94448-08-5
3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

Guidance literature:: With acetic acid; In ethanol; for 2h; Ambient temperature;
DOI:10.1248/cpb.32.3724

Reference yield:

: 2483-56-9,89464-41-5
5,5-dimethyltetramic acid

: 94448-08-5
3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-toluenesulfonic acid monohydrate / benzene / Heating

2: 78 percent / acetic acid / ethanol / 2 h / Ambient temperature

With toluene-4-sulfonic acid; acetic acid; In ethanol; benzene;
DOI:10.1248/cpb.32.3724

Reference yield:

: 94447-93-5
5,5-Dimethyl-2,4-dioxo-pyrrolidine-3-carboxylic acid ethyl ester

: 94448-08-5
3,3-dimethyl-10-(3',4'-dimethoxyphenyl)-3,4,9,10-tetrahydro-1H-pyrrolo<3,4-b><1,5>benzodiazepin-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / nitromethane / 0.58 h / Heating

2: 93 percent / p-toluenesulfonic acid monohydrate / benzene / Heating

3: 78 percent / acetic acid / ethanol / 2 h / Ambient temperature

With water; toluene-4-sulfonic acid; acetic acid; In nitromethane; ethanol; benzene;
DOI:10.1248/cpb.32.3724