[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

Base Information

Chemical Name:[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane
CAS No.:183236-39-7
Molecular Formula:C₂₇H₃₉N₉O₄Si
Molecular Weight:581.75
Hs Code.:

Synonyms:[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

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Chemical Property of [3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

Chemical Property:

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Technology Process of [3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

There total 6 articles about [3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid 2-[3-(tert-butyl-diphenyl-silanyloxy)-2,2-bis-(2-methanesulfonyloxy-ethoxymethyl)-propoxy]-ethyl ester

: 183236-39-7
[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 130 ℃; for 5h; Yield given;
DOI:10.1139/v96-191

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 183236-39-7
[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / imidazole / dimethylformamide / 24 h / 0 - 15 °C

2: 66 percent / 60percent NaH / dimethylformamide / Ambient temperature

3: O₃ / methanol; CH₂Cl₂ / -78 °C

4: NaBH₄ / ethanol / 24 h / Ambient temperature

5: pyridine / 4 h / 25 °C

6: NaN₃ / dimethylformamide / 5 h / 130 °C

With 1H-imidazole; sodium tetrahydroborate; sodium azide; sodium hydride; ozone; In pyridine; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1139/v96-191

Reference yield:

: 183236-36-4
2-<<(tert-butyldiphenylsilyl)oxy>methyl>-2-(hydroxymethyl)-1,3-propanediol

: 183236-39-7
[3-(2-Azido-ethoxy)-2,2-bis-(2-azido-ethoxymethyl)-propoxy]-tert-butyl-diphenyl-silane

Guidance literature:: Multi-step reaction with 5 steps

1: 66 percent / 60percent NaH / dimethylformamide / Ambient temperature

2: O₃ / methanol; CH₂Cl₂ / -78 °C

3: NaBH₄ / ethanol / 24 h / Ambient temperature

4: pyridine / 4 h / 25 °C

5: NaN₃ / dimethylformamide / 5 h / 130 °C

With sodium tetrahydroborate; sodium azide; sodium hydride; ozone; In pyridine; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1139/v96-191