Benzenemethanol,a-(aminomethyl)-4-methoxy-,(S)-

Base Information

• Chemical Name: Benzenemethanol,a-(aminomethyl)-4-methoxy-,(S)-
• CAS No.: 46084-19-9
• Molecular Formula: C9H13 N O2
• Molecular Weight: 167.208
• Hs Code.: 2922509090
• Mol file: 46084-19-9.mol

Synonyms:Benzenemethanol,a-(aminomethyl)-4-methoxy-, (S)-

Chemical Property of Benzenemethanol,a-(aminomethyl)-4-methoxy-,(S)-

Chemical Property:

• Vapor Pressure: 9.43E-05mmHg at 25°C
• Boiling Point: 325.4°C at 760 mmHg
• Flash Point: 150.6°C
• PSA: 55.48000
• Density: 1.128g/cm³
• LogP: 1.38760

Purity/Quality:

98% ^*data from raw suppliers

(S)-2-Amino-1-(4-methoxyphenyl)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: Pd nanoparticle-catalyzed reduction to (S)-2-Amino-1-(4-methoxyphenyl)ethanol used for the enantioselective synthesis of pure 1,2-amino alcohols.

Technology Process of Benzenemethanol,a-(aminomethyl)-4-methoxy-,(S)-

There total 20 articles about Benzenemethanol,a-(aminomethyl)-4-methoxy-,(S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(S)-(+)-2-azido-1-(4-methoxyphenyl)-1-ethanol (297765-47-0) → (S)-(+)-2-amino-1-(4-methoxyphenyl)-1-ethanol (46084-19-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 3h; under 760 Torr;

DOI:10.1016/j.tetasy.2004.11.013

Reference yield: 86.0%

(S)-(+)-[2-hydroxy-2-(4-methoxy-phenyl)-ethyl]-carbamic acid benzyl ester (178888-43-2) → (S)-(+)-2-amino-1-(4-methoxyphenyl)-1-ethanol (46084-19-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 8h; under 760 Torr;

DOI:10.1021/ja038043d

Reference yield: 86.0%

→ (S)-(+)-2-amino-1-(4-methoxyphenyl)-1-ethanol (46084-19-9)

Guidance literature:

upstream raw materials:

(R)-(+)-α-<(tert-butyldimethylsilyl)oxy>-4-methoxybenzeneacetonitrile

2-acetamido-1-(4-methoxyphenyl)ethyl acetate

(S)-(+)-[2-hydroxy-2-(4-methoxy-phenyl)-ethyl]-carbamic acid benzyl ester

(S)-(+)-2-azido-1-(4-methoxyphenyl)-1-ethanol

Downstream raw materials:

(S)-N-[2-hydroxy-2-(4-methoxyphenyl)ethyl]benzamide

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