16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

Base Information

Chemical Name:16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate
CAS No.:143634-84-8
Molecular Formula:BF₄*C₃₇H₃₆NO₅
Molecular Weight:661.501
Hs Code.:

Synonyms:16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

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Chemical Property of 16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

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Technology Process of 16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

There total 8 articles about 16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 448-61-3
2,4,6-triphenylpyrylium tetrafluoroborate

: 132699-11-7
16-Amino-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol

: 143634-84-8
16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

Guidance literature:: With acetic acid; In dichloromethane; for 4h;

Reference yield:

: 65112-35-8
3,6,9,12-Tetraoxabicyclo[12.3.1]octadeca-1⁽¹⁸⁾,14,16-trien-18-ol

: 143634-84-8
16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / KNO₂, concd. HNO₃ / H₂O / 0.67 h / Ambient temperature

2: 99 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Ambient temperature

3: 82 percent / AcOH / CH₂Cl₂ / 4 h / Ambient temperature

With potassium nitrite; hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In methanol; dichloromethane; water;

Reference yield:

: 65112-33-6
18-Methoxy-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-triene

: 143634-84-8
16-(2,4,6-Triphenyl-1-pyridinio)-3,6,9,12-tetraoxabicyclo<12.3.1>octadeca-1(18),14,16-trien-18-ol Tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / anhydr. LiI / pyridine / 8 h / Heating

2: 86 percent / KNO₂, concd. HNO₃ / H₂O / 0.67 h / Ambient temperature

3: 99 percent / H₂ / 10percent Pd/C / methanol / 760 Torr / Ambient temperature

4: 82 percent / AcOH / CH₂Cl₂ / 4 h / Ambient temperature

With potassium nitrite; hydrogen; nitric acid; acetic acid; lithium iodide; palladium on activated charcoal; In pyridine; methanol; dichloromethane; water;