Technology Process of C45H59NO18
There total 5 articles about C45H59NO18 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C60H81NO20Si;
With
pyridine; hydrogen fluoride;
In
acetonitrile;
at 20 ℃;
for 2h;
With
methanol; acetyl chloride;
In
dichloromethane;
at 20 ℃;
DOI:10.1016/j.bmcl.2005.08.066
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 76 percent / Et4N(BH4) / methanol / 2.5 h / -40 - 0 °C
2.1: DMAP; EDCI / CH2Cl2 / 1.5 h / 20 °C
3.1: HF; pyridine / acetonitrile / 2 h / 20 °C
3.2: 248 mg / AcCl; MeOH / CH2Cl2 / 20 °C
With
pyridine; dmap; hydrogen fluoride; tetraethylammonium borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.08.066
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 230 mg / imidazole / CH2Cl2 / 1.5 h / 40 °C
2.1: 76 percent / Et4N(BH4) / methanol / 2.5 h / -40 - 0 °C
3.1: DMAP; EDCI / CH2Cl2 / 1.5 h / 20 °C
4.1: HF; pyridine / acetonitrile / 2 h / 20 °C
4.2: 248 mg / AcCl; MeOH / CH2Cl2 / 20 °C
With
pyridine; 1H-imidazole; dmap; hydrogen fluoride; tetraethylammonium borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2005.08.066