Technology Process of C26H41NO6S
There total 6 articles about C26H41NO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 0 ℃;
DOI:10.1002/psc.1376
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium chloride / tetrahydrofuran / 24 h / 0 - 20 °C
2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 °C
2.2: 8 h / -78 °C
3.1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 20 °C
4.1: dmap; triethylamine / dichloromethane / 0 °C
With
dmap; lithium aluminium tetrahydride; sodium hexamethyldisilazane; triethylamine; lithium chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
2.1: Evans' asymmetric alkylation / 2.2: Evans' asymmetric alkylation;
DOI:10.1002/psc.1376
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 - 20 °C
2: dmap; triethylamine / dichloromethane / 0 °C
With
dmap; lithium aluminium tetrahydride; triethylamine;
In
diethyl ether; dichloromethane;
DOI:10.1002/psc.1376