3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

Base Information

Chemical Name:3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester
CAS No.:107223-09-6
Molecular Formula:C₃₅H₄₄N₄O₁₂
Molecular Weight:712.754
Hs Code.:

3-O-Benzyl-6-<O-benzyl-N-(tert-butyloxycarbonyl)-L-serylamino>-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

Synonyms:3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

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Chemical Property of 3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

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Technology Process of 3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

There total 5 articles about 3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 13650-73-2
2,5-dioxopyrrolidin-1-yl O-benzyl-N-t-butoxycarbonyl-L-serinate

: 107223-08-5
6-Amino-3-O-benzyl-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

: 107223-09-6
3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; for 18h; 0 deg C to room temp.;

Reference yield:

: 107244-49-5
3-O-Benzyl-6-(benzyloxycarbonylamino)-1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

: 107223-09-6
3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / 0.1N HCl, H₂ / 10percent Pd/C / methanol / 1.5 h

2: 78 percent / NaHCO₃ / tetrahydrofuran; H₂O / 18 h / 0 deg C to room temp.

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water;

Reference yield:

: 107223-06-3
2,5-Di-O-acetyl-3-O-benzyl-6-(benzyloxycarbonylamino)-1,6-didesoxy-1-<3,4-dihydro-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

: 107223-09-6
3-O-Benzyl-6--1,6-didesoxy-1-<3,4-dihydro-3-methyl-2,4-dioxo-1(2H)-pyrimidinyl>-L-glycero-α-L-ido-heptofuranuronsaeure-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / methanol; diethyl ether

2: 98 percent / 1M MeONa / methanol / 5 h / Ambient temperature

3: 89 percent / 0.1N HCl, H₂ / 10percent Pd/C / methanol / 1.5 h

4: 78 percent / NaHCO₃ / tetrahydrofuran; H₂O / 18 h / 0 deg C to room temp.

With hydrogenchloride; hydrogen; sodium methylate; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; water;