1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

Base Information

Chemical Name:1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide
CAS No.:95702-51-5
Molecular Formula:C₂₁H₂₄N₆OS
Molecular Weight:408.527
Hs Code.:

1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1<i>H</i>-pyrazol-4-yl)-thiosemicarbazide

Synonyms:1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

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Chemical Property of 1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

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Technology Process of 1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

There total 4 articles about 1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 96447-49-3
4-(2,3-dimethyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrazol-4-yl)thiosemicarbazide

: 100-10-7
4-dimethylamino-benzaldehyde

: 95702-51-5
1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

Guidance literature:: In butan-1-ol; for 1h; Heating;

Reference yield:

: 83-07-8
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one

: 95702-51-5
1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: NH₄OH / 1 h / Ambient temperature

2: N₂H₄*H₂O / 3 h / Heating

3: 87 percent / butan-1-ol / 1 h / Heating

With ammonium hydroxide; hydrazine hydrate; In butan-1-ol;

Reference yield:

: (1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-dithiocarbamic acid; compound with ammonia

: 95702-51-5
1-(4-dimethylamino-benzylidene)-4-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O / 3 h / Heating

2: 87 percent / butan-1-ol / 1 h / Heating

With hydrazine hydrate; In butan-1-ol;