sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Base Information

Chemical Name:sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate
CAS No.:123226-88-0
Molecular Formula:C₂₄H₂₂NO₅S₂*Na
Molecular Weight:491.564
Hs Code.:

Synonyms:sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Suppliers and Price of sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

There total 7 articles about sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55689-64-0
methyl 6,11-dihydro-11-oxodibenz[b,e]oxepin-2-acetate

: 123226-88-0
sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / methanol

2: p-toluenesulfonic acid

3: BF₃*Et₂O / CH₂Cl₂ / 3 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

5: 10 N aq. NaOH / H₂O; methanol / 2.5 h / Heating

With sodium hydroxide; sodium tetrahydroborate; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/jm00096a016

Reference yield:

: 123226-65-3
[11-(2-Benzenesulfonylamino-ethylsulfanyl)-6,11-dihydro-dibenzo[b,e]oxepin-2-yl]-acetic acid methyl ester

: 123226-88-0
sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Guidance literature:: With sodium hydroxide; In methanol; water; for 2.5h; Heating;
DOI:10.1021/jm00096a016

Reference yield:

: 56427-50-0
methyl 6,11-dihydro-11-hydroxydibenz[b,e]oxepin-2-acetate

: 123226-88-0
sodium 11-[2-[(phenylsulfonyl)amino]ethyl]thio-6,11-dihydrodibenz[b,e]oxepin-2-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: p-toluenesulfonic acid

2: BF₃*Et₂O / CH₂Cl₂ / 3 h / Ambient temperature

3: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

4: 10 N aq. NaOH / H₂O; methanol / 2.5 h / Heating

With sodium hydroxide; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/jm00096a016