2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

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Chemical Name:2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine
CAS No.:1584055-90-2
Molecular Formula:C₃₃H₄₉N₇O₇
Molecular Weight:655.795
Hs Code.:

Synonyms:2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

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Chemical Property of 2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

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Technology Process of 2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

There total 4 articles about 2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393922-29-6
2-N-(2-aminoethyl)-4-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazine-2,4-diamine

: 101834-30-4
2-(10β-dihydroartemisinoxy)propyl bromide

: 1584055-90-2
2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 0.0666667h; Microwave irradiation;
DOI:10.1016/j.ejmech.2014.01.040

Reference yield:

: 21665-63-4
4-chloro-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-1,3,5-triazin-2-amine

: 1584055-90-2
2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 50 - 70 °C

2: potassium carbonate / N,N-dimethyl-formamide / 0.07 h / 50 °C / Microwave irradiation

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.01.040

Reference yield:

: 30377-27-6
4,6-dichloro-N-(4-methoxyphenyl)-1,3,5-triazin-2-amine

: 1584055-90-2
2-N-(4-methoxyphenyl)-6-(morpholin-4-yl)-4-N-{2-[(2-{10β dihydroartemisinoxy}ethyl)amino]ethyl}-1,3,5-triazine-2,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / acetone / 0 - 20 °C

2: 50 - 70 °C

3: potassium carbonate / N,N-dimethyl-formamide / 0.07 h / 50 °C / Microwave irradiation

With sodium carbonate; potassium carbonate; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2014.01.040