(4-methylpent-1-yl)triphenylphosphonium iodide

Base Information

Chemical Name:(4-methylpent-1-yl)triphenylphosphonium iodide
CAS No.:117940-59-7
Molecular Formula:C₂₄H₂₈P*I
Molecular Weight:474.365
Hs Code.:

Synonyms:(4-methylpent-1-yl)triphenylphosphonium iodide

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Chemical Property of (4-methylpent-1-yl)triphenylphosphonium iodide

Chemical Property:

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Technology Process of (4-methylpent-1-yl)triphenylphosphonium iodide

There total 2 articles about (4-methylpent-1-yl)triphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 6196-80-1
1-iodo-4-methylpentane

: 603-35-0
triphenylphosphine

: 117940-59-7
(4-methylpent-1-yl)triphenylphosphonium iodide

Guidance literature:: In acetonitrile; for 16h; Heating;
DOI:10.1021/ja00184a035

Reference yield:

: 4-methylpentyl 4-methylbenzenesulfonate

: 117940-59-7
(4-methylpent-1-yl)triphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 24 h / Ambient temperature

2: acetonitrile / 16 h / Heating

With sodium iodide; In acetone; acetonitrile;
DOI:10.1021/ja00184a035

Reference yield:

: 117940-59-7
(4-methylpent-1-yl)triphenylphosphonium iodide

: 55830-20-1
2-methyloctadecan-8-one

: 54910-51-9
(2S-cis)-7,8-epoxy-2-methyloctadecane

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / 1.) THF, hexane, -78 deg C, 2 h, 2.) 3 h

2: hydrogen / Wilkinson's catalyst / benzene / 3 h

With n-butyllithium; hydrogen; Wilkinson's catalyst; In benzene;
DOI:10.1021/ja00184a035