2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

Base Information

Chemical Name:2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid
CAS No.:1397694-65-3
Molecular Formula:C₁₅H₁₆O₅
Molecular Weight:276.289
Hs Code.:

Synonyms:2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

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Chemical Property of 2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

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Technology Process of 2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

There total 5 articles about 2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₆O₄

: 1397694-65-3
2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; dihydrogen peroxide; In water; acetonitrile; at 10 - 20 ℃; for 4h;
DOI:10.1016/j.tet.2012.07.020

Reference yield:

: ethyl 6,7-dihydroxy-3-(4-methoxy-3-methylphenyl)-2-methylhept-3-enoate

: 1397694-65-3
2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / toluene; acetonitrile / 72 h / 0 - 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C / Inert atmosphere

3: sodium periodate / water; acetone / 0.25 h / 0 - 20 °C

4: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 4 h / 10 - 20 °C

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; boron trifluoride diethyl etherate; water; dihydrogen peroxide; 4-methylmorpholine N-oxide; In dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1016/j.tet.2012.07.020

Reference yield:

: 1397694-70-0
5-(2,3-dihydroxypropyl)-4-(4-methoxy-3-methylphenyl)-3-methylfuran-2(5H)-one

: 1397694-65-3
2-(3-(4-methoxy-3-methylphenyl)-4-methyl-5-oxo-2,5-dihydrofuran-2-yl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium periodate / water; acetone / 0.25 h / 0 - 20 °C

2: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / water; acetonitrile / 4 h / 10 - 20 °C

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; dihydrogen peroxide; In water; acetone; acetonitrile;
DOI:10.1016/j.tet.2012.07.020