5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

Base Information

Chemical Name:5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin
CAS No.:689278-58-8
Molecular Formula:C₂₅H₂₇ClN₂O₁₀S
Molecular Weight:583.016
Hs Code.:

Synonyms:5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

Suppliers and Price of 5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

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Technology Process of 5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

There total 1 articles about 5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 79851-71-1
5-(4-chlorobenzylidene)-3-methyl-2-thiohydantoin

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 689278-58-8
5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

Guidance literature:: With potassium hydroxide; In acetone; at 20 ℃; for 4h;
DOI:10.1080/10426500490257131

Reference yield:

: 689278-58-8
5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

: 79851-71-1
5-(4-chlorobenzylidene)-3-methyl-2-thiohydantoin

: 14745-12-1
5-(4-chlorobenzylidene)-3-methylhydantoin

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 24h;
DOI:10.1080/10426500490257131

Reference yield:

: 689278-58-8
5-(4-chlorobenzylidene)-3-methyl-2-(2',3',4',6'-tetra-O-acetyl-β-D-thioglucopyranosyl)hydantoin

: Acetic acid (2R,3S,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-{4-[1-(4-chloro-phenyl)-meth-(E)-ylidene]-1-methyl-5-oxo-4,5-dihydro-1H-imidazol-2-ylsulfanyl}-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.79 g / NH₃ / methanol / 24 h / 20 °C

2: 89 percent / aq. KOH / acetone / 20 h / 20 °C

With potassium hydroxide; ammonia; In methanol; acetone;
DOI:10.1080/10426500490257131