3,4-dihydroxy-2,5-dimethylbenzaldehyde

Base Information

Chemical Name:3,4-dihydroxy-2,5-dimethylbenzaldehyde
CAS No.:97073-42-2
Molecular Formula:C₉H₁₀O₃
Molecular Weight:166.177
Hs Code.:

Synonyms:3,4-dihydroxy-2,5-dimethylbenzaldehyde

Suppliers and Price of 3,4-dihydroxy-2,5-dimethylbenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,4-dihydroxy-2,5-dimethylbenzaldehyde

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3,4-dihydroxy-2,5-dimethylbenzaldehyde

There total 5 articles about 3,4-dihydroxy-2,5-dimethylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2785-78-6
3,6-Dimethylcatechol

: 122-51-0
orthoformic acid triethyl ester

: 97073-42-2
3,4-dihydroxy-2,5-dimethylbenzaldehyde

Guidance literature:: With aluminium trichloride; In benzene; at 60 ℃; for 0.333333h;
DOI:10.1021/jm00147a027

Reference yield:

: 95-87-4
2,5-Dimethylphenol

: 97073-42-2
3,4-dihydroxy-2,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium chloride; triethylamine / acetonitrile / 3 h / 100 °C

2: dihydrogen peroxide; sodium hydroxide; water / tetrahydrofuran / 0.25 h / 20 °C

3: aluminum (III) chloride / toluene / 3 h / 60 °C

With aluminum (III) chloride; water; dihydrogen peroxide; triethylamine; sodium hydroxide; magnesium chloride; In tetrahydrofuran; toluene; acetonitrile; 2: |Dakin Phenol Oxidation;
DOI:10.1039/C7RA02329D

Reference yield:

: 1666-04-2
2-hydroxy-3,6-dimethylbenzaldehyde

: 97073-42-2
3,4-dihydroxy-2,5-dimethylbenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sodium hydroxide; water / tetrahydrofuran / 0.25 h / 20 °C

2: aluminum (III) chloride / toluene / 3 h / 60 °C

With aluminum (III) chloride; water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; toluene; 1: |Dakin Phenol Oxidation;
DOI:10.1039/C7RA02329D