Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester

Base Information

• Chemical Name: Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester
• CAS No.: 73092-79-2
• Molecular Formula: C13H9 Cl O3
• Molecular Weight: 248.66
• Mol file: 73092-79-2.mol

Synonyms:Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester

Chemical Property of Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 417.586°C at 760 mmHg
• Flash Point: 206.349°C
• PSA: 46.53000
• Density: 1.357g/cm³
• LogP: 3.26480

Purity/Quality:

98% ^*data from raw suppliers

4-CHLORO-BENZOIC ACID-4-HYDROXYPHENYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester

There total 3 articles about Benzoic acid, 4-chloro-, 4-hydroxyphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

4-chlorobenzaldehyde (104-88-1) + p-benzoquinone (106-51-4) → 4-hydroxyphenyl 4-chlorobenzoate (73092-79-2)

Guidance literature:

With tert.-butylhydroperoxide; copper(II) acetate monohydrate; In water; dimethyl sulfoxide; at 100 - 110 ℃; for 24h; Sealed tube;

DOI:10.1021/acs.joc.5b02175

Reference yield: 56.0%

para-Chlorobenzyl alcohol (873-76-7) + p-benzoquinone (106-51-4) → 4-hydroxyphenyl 4-chlorobenzoate (73092-79-2)

Guidance literature:

With tert.-butylhydroperoxide; copper(II) acetate monohydrate; In water; dimethyl sulfoxide; at 100 - 110 ℃; for 24h; Sealed tube;

DOI:10.1021/acs.joc.5b02175

Reference yield:

→ 4-hydroxyphenyl 4-chlorobenzoate (73092-79-2)

Guidance literature:

Aus 4-Chlor-benzoylchlorid und Hydrochinon;

upstream raw materials:

4-chlorobenzaldehyde

p-benzoquinone

para-Chlorobenzyl alcohol

Refernces