(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

Base Information

Chemical Name:(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione
CAS No.:1192030-86-6
Molecular Formula:C₄₀H₄₀O₅Si
Molecular Weight:628.84
Hs Code.:

Synonyms:(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

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Chemical Property of (3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

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Technology Process of (3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

There total 1 articles about (3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₂O₅Si

: 1192030-86-6
(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In acetonitrile; at 50 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ja9073694

Reference yield: 49.0%

: 1192030-59-3
4-bromo-9,10-dimethoxy-8-(methoxymethoxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

: 1192030-86-6
(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

: 1192159-96-8
C₅₉H₆₁BrO₁₀Si

Guidance literature:: 4-bromo-9,10-dimethoxy-8-(methoxymethoxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;

(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione; With di-n-butylboryl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja9073694

Reference yield: 31.0%

: 1192030-57-1
9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one

: 1192030-86-6
(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione

: 1192030-72-0
C₆₅H₆₆O₁₀Si

Guidance literature:: 9,10-dimethoxy-8-(4-methoxybenzyloxy)-6-methyl-3,4-dihydroanthracen-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(3R,4R)-8-(benzyloxy)-4-((S)-1-(tert-butyldiphenylsilyloxy)ethyl)-3-methyl-3,4-dihydro-anthracene-1,9,10(2H)-trione; In tetrahydrofuran; at -78 - 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja9073694