(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

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Chemical Name:(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester
CAS No.:202145-89-9
Molecular Formula:C₃₀H₃₆F₆N₄O₆
Molecular Weight:662.629
Hs Code.:

Synonyms:(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

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Chemical Property of (4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

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Technology Process of (4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

There total 1 articles about (4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: N¹,N¹⁴-bis(trifluoroacetyl)spermine ditrifluoroacetate

: 202145-89-9
(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 1h;
DOI:10.1016/S0968-0896(97)00157-0

Reference yield: 91.0%

: 202145-89-9
(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

: 174654-04-7
(3-Amino-propyl)-{4-[(3-amino-propyl)-benzyloxycarbonyl-amino]-butyl}-carbamic acid benzyl ester

Guidance literature:: With ammonium hydroxide; In methanol; Heating;
DOI:10.1016/S0968-0896(97)00157-0

Reference yield:

: 202145-89-9
(4-{Benzyloxycarbonyl-[3-(2,2,2-trifluoro-acetylamino)-propyl]-amino}-butyl)-[3-(2,2,2-trifluoro-acetylamino)-propyl]-carbamic acid benzyl ester

: 119493-76-4
N,N'-bis-(3-benzylaminopropyl)butane-1,4-diamine

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / NH₃ aq. / methanol / Heating

2: ethanol / 5 h / Ambient temperature

3: NaBH₄ / ethanol / 1 h / 0 °C

4: 46 percent / H₂ / 5percent Pd/C / ethanol / 2585.7 Torr

With ammonium hydroxide; sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1016/S0968-0896(97)00157-0