2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

Base Information

Chemical Name:2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole
CAS No.:1421922-75-9
Molecular Formula:C₂₀H₂₀N₂O₃S
Molecular Weight:368.456
Hs Code.:

Synonyms:2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

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Chemical Property of 2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

Chemical Property:

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Technology Process of 2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

There total 6 articles about 2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-44-5
p-cresol

: 1421922-74-8
4-(bromomethyl)-2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazole

: 1421922-75-9
2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

Guidance literature:: With potassium carbonate; In acetone; for 9h; Reflux;

Reference yield:

: 1421922-73-7
[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]methanol

: 1421922-75-9
2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

Guidance literature:: Multi-step reaction with 2 steps

1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

2: potassium carbonate / acetone / 9 h / Reflux

With carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; acetone;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421922-75-9
2-(2,5-dimethyl-4-nitrobenzyl)-4-[(4-methylphenoxy)methyl]-1,3-thiazole

Guidance literature:: Multi-step reaction with 6 steps

1: nitric acid / 0.5 h / Cooling with ice

2: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3: triethylamine / isopropyl alcohol / 4 h / 80 °C

4: sodium methylate; methanol / 0.5 h / Cooling with ice

5: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

6: potassium carbonate / acetone / 9 h / Reflux

With hydrogenchloride; methanol; carbon tetrabromide; nitric acid; sodium methylate; potassium carbonate; O,O-Diethyl hydrogen phosphorodithioate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethyl acetate; isopropyl alcohol; acetone;