2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1130728-72-1
Molecular Formula:C₁₆H₂₅BO₄
Molecular Weight:292.183
Hs Code.:

Synonyms:2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 2 articles about 2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1130728-51-6
(2,5-dimethyl-3,6-dimethoxylphenyl)boronic acid

: 1130728-72-1
2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: In pentane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.200803428

Reference yield: 79.0%

: 1130728-51-6
(2,5-dimethyl-3,6-dimethoxylphenyl)boronic acid

: 67975-91-1
2-chloro-4,4,5,5,-tetramethyl-1,3,2-dioxaboralane

: 1130728-72-1
2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: In pentane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c7ob00979h

Reference yield:

: 1130728-72-1
2-(3,6-dimethoxy-2,4-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 527-61-7
2,6-dimethyl-1,4-benzoquinone

: 3,5-dimethyl-2-(3-oxobutyl)cyclohexa-2,5-diene-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium cerium (IV) nitrate / acetonitrile; water / 0.5 h

2: chloro(1,5-cyclooctadiene)rhodium(I) dimer; triphenylphosphine / water; isopropyl alcohol; acetone / 16 h / 60 °C / Inert atmosphere

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; ammonium cerium (IV) nitrate; triphenylphosphine; In water; isopropyl alcohol; acetone; acetonitrile;
DOI:10.1039/c7ob00979h