(2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

Base Information

Chemical Name:(2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone
CAS No.:743430-43-5
Molecular Formula:C₂₁H₂₅NO₅
Molecular Weight:371.433
Hs Code.:

Synonyms:(2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

Chemical Property:

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Technology Process of (2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

There total 2 articles about (2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177896-09-2
tert-butyl benzylidenecarbamate

: 224321-19-1
2-hydroxy-1-(2-methoxyphenyl)ethanone

: [(1R,2R)-2-Hydroxy-3-(2-methoxy-phenyl)-3-oxo-1-phenyl-propyl]-carbamic acid tert-butyl ester

: [(1S,2S)-2-Hydroxy-3-(2-methoxy-phenyl)-3-oxo-1-phenyl-propyl]-carbamic acid tert-butyl ester

: 743430-43-5
(2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

Guidance literature:: With 1,1'-bis[(S,S)-BINOL-3-yl]dimethyl ether; 3 A molecular sieve; diethylzinc; In tetrahydrofuran; diethyl ether; hexane; at -40 ℃; for 36h;
DOI:10.1021/ja0482435

Reference yield:

: 177896-09-2
tert-butyl benzylidenecarbamate

: 224321-19-1
2-hydroxy-1-(2-methoxyphenyl)ethanone

: [(1R,2R)-2-Hydroxy-3-(2-methoxy-phenyl)-3-oxo-1-phenyl-propyl]-carbamic acid tert-butyl ester

: 743430-43-5
(2R,3S)-2-hydroxy-1-(2-methoxyphenyl)-3-(N-tert-butoxycarbonylamino)-3-phenyl-1-propanone

Guidance literature:: With 1,1'-bis[(S,S)-BINOL-3-yl]dimethyl ether; 3 A molecular sieve; diethylzinc; In tetrahydrofuran; hexane; at -20 ℃; Kinetics;
DOI:10.1021/ja0482435