3-methyl-1-phenethylpiperidine

Base Information

• Chemical Name: 3-methyl-1-phenethylpiperidine
• CAS No.: 3469-94-1
• Molecular Formula: C₁₄H₂₁N
• Molecular Weight: 203.327

Synonyms:3-methyl-1-phenethylpiperidine

Chemical Property of 3-methyl-1-phenethylpiperidine

Chemical Property:

Purity/Quality:

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Technology Process of 3-methyl-1-phenethylpiperidine

There total 4 articles about 3-methyl-1-phenethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3-Methylpiperidine (626-56-2,53152-98-0) → 3-methyl-1-phenethylpiperidine (3469-94-1)

Guidance literature:

With C₁₉H₄₃KMgN₂Si₄; In neat (no solvent); at 60 ℃; for 12h; Sealed tube;

DOI:10.1016/j.jorganchem.2022.122254

Reference yield:

3-methyl-1-[(E)-2-phenylethenyl]piperidine → 3-methyl-1-phenethylpiperidine (3469-94-1)

Guidance literature:

With sodium cyanoborohydride; acetic acid; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1039/c5cc02677f

Reference yield:

3-Methylpiperidine (626-56-2,53152-98-0) → 3-methyl-1-phenethylpiperidine (3469-94-1)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(01)00788-0

upstream raw materials:

3-Methylpiperidine

phenylacetylene

styrene

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