benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

Base Information

Chemical Name:benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate
CAS No.:642410-53-5
Molecular Formula:C₃₃H₄₉NO₇S
Molecular Weight:603.821
Hs Code.:

Synonyms:benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

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Chemical Property of benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

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Technology Process of benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

There total 1 articles about benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 96550-93-5
(decane-1-sulfonyl)benzene

: (S)-2-(1-Ethoxy-ethoxymethyl)-5-oxo-pyrrolidine-1-carboxylic acid benzyl ester

: 2-benzenesulfonyl-undecanoic acid benzyl ester

: 642410-53-5
benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -72 ℃;
DOI:10.1002/ejoc.200300393

Reference yield: 92.0%

: 642410-53-5
benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

: 642410-60-4
benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxotetradecylcarbamate

Guidance literature:: With sodium amalgam; camphor-10-sulfonic acid; In methanol; at 20 ℃;
DOI:10.1002/ejoc.200300393

Reference yield:

: 642410-53-5
benzyl (1S)-1-[(1-ethoxyethoxy)methyl]-4-oxo-5-(phenylsulfonyl)tetradecylcarbamate

: 642410-75-1
(2S,5S)-N-(benzyloxycarbonyl)-5-decyl-2-(hydroxymethyl)pyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 92 percent / sodium amalgam; NaHPO₄ / methanol / 20 °C

2.1: 68 percent / H₂ / Pd(OH)2 / methanol / 20 °C / 760 Torr

3.1: aq. HCl / tetrahydrofuran / 20 °C

3.2: 60 mg / Na₂CO₃ / CH₂Cl₂; H₂O

With hydrogenchloride; sodium amalgam; camphor-10-sulfonic acid; hydrogen; palladium dihydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/ejoc.200300393