(E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine

Base Information

• Chemical Name: (E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine
• CAS No.: 149833-55-6
• Molecular Formula: C₁₃H₉ClN₄O₄
• Molecular Weight: 320.692

Synonyms:(E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine

Chemical Property of (E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine

Chemical Property:

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Technology Process of (E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine

There total 10 articles about (E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

4-chlorobenzaldehyde (104-88-1) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 4-chloro-benzaldehyde-(2,4-dinitro-phenylhydrazone) (149833-55-6,1773-47-3)

Guidance literature:

With oxidized single-walled carbon nanotubes(SWCNs-COOH); In ethanol; at 80 ℃; for 0.5h;

Reference yield: 93.0%

N-(p-chlorobenzylideneamino)phthalimide (34403-64-0) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 4-chloro-benzaldehyde-(2,4-dinitro-phenylhydrazone) (149833-55-6,1773-47-3)

Guidance literature:

In ethanol; for 0.0833333h; Heating;

Reference yield: 90.0%

4-chlorobenzaldehyde (104-88-1) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → (E)-1-(4-chlorobenzylidene)-2-(2,4-dinitro phenyl)hydrazine (149833-55-6)

Guidance literature:

With sulfuric acid; In ethanol; at 20 ℃; for 1h;

DOI:10.4067/S0717-97072016000300015

upstream raw materials:

4-chlorobenzaldehyde

(2,4-dinitro-phenyl)-hydrazine

N-(p-chlorobenzylideneamino)phthalimide

para-Chlorobenzyl alcohol

Downstream raw materials:

4-chlorobenzaldehyde

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