N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Name:N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide
CAS No.:946612-28-8
Molecular Formula:C₄₀H₂₂F₄N₂O₄
Molecular Weight:670.619
Hs Code.:

Synonyms:N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Property of N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

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Technology Process of N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

There total 3 articles about N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 946612-29-9
N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid bisimide

: 946612-28-8
N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: With potassium fluoride; 1,3-dimethyl-2-(N',N',N",N"-tetramethylguanidino)-4,5-dihydro-3H-imidazolium chloride; In sulfolane; at 160 ℃; for 5h; Inert atmosphere;
DOI:10.1515/znb-2009-0621

Reference yield:

: 156028-26-1
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride

: 946612-28-8
N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: zinc diacetate / quinoline / 4 h / 180 °C

2: potassium fluoride; 1,3-dimethyl-2-(N',N',N",N"-tetramethylguanidino)-4,5-dihydro-3H-imidazolium chloride / sulfolane / 5 h / 160 °C

With potassium fluoride; zinc diacetate; 1,3-dimethyl-2-(N',N',N",N"-tetramethylguanidino)-4,5-dihydro-3H-imidazolium chloride; In quinoline; sulfolane;

Reference yield:

: 103-67-3
benzyl-methyl-amine

: 946612-28-8
N,N'-bis(α-methylbenzyl)-1,6,7,12-tetrafluoroperylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: zinc diacetate / quinoline / 4 h / 180 °C

2: potassium fluoride; 1,3-dimethyl-2-(N',N',N",N"-tetramethylguanidino)-4,5-dihydro-3H-imidazolium chloride / sulfolane / 5 h / 160 °C

With potassium fluoride; zinc diacetate; 1,3-dimethyl-2-(N',N',N",N"-tetramethylguanidino)-4,5-dihydro-3H-imidazolium chloride; In quinoline; sulfolane;