N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV)

Base Information

Chemical Name:N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV)
CAS No.:1426302-15-9
Molecular Formula:C₂₉H₄₄Cl₃N₃Ti
Molecular Weight:588.927
Hs Code.:

Synonyms:N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV)

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Chemical Property of N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV)

Chemical Property:

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Technology Process of N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV)

There total 5 articles about N',N-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichloridotitanium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 684-55-9
diethylamidotrichloridotitanium(IV)

: 2162-74-5
N,N'-bis(2,6-diisopropylphenyl)carbodiimide

: 1426302-15-9
N',N''-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichlorido titanium(IV)

Guidance literature:: In toluene; at 50 - 110 ℃; Inert atmosphere;
DOI:10.1002/chem.201202506

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1426302-15-9
N',N''-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichlorido titanium(IV)

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / water / Inert atmosphere; Schlenk technique

2: triethylamine; triphenylphosphine / tetrachloromethane; dichloromethane / Inert atmosphere; Schlenk technique

3: toluene / Inert atmosphere; Schlenk technique

With triethylamine; triphenylphosphine; In tetrachloromethane; dichloromethane; water; toluene;
DOI:10.1002/ejic.201301610

Reference yield:

: 25348-97-4
N,N'-bis(2,6-diisopropylphenyl)thiourea

: 1426302-15-9
N',N''-bis(2,6-diisopropylphenyl)-N,N-diethylguanidinatotrichlorido titanium(IV)

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; triphenylphosphine / tetrachloromethane; dichloromethane / Inert atmosphere; Schlenk technique

2: toluene / Inert atmosphere; Schlenk technique

With triethylamine; triphenylphosphine; In tetrachloromethane; dichloromethane; toluene;
DOI:10.1002/ejic.201301610