nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

Base Information

Chemical Name:nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester
CAS No.:185063-20-1
Molecular Formula:C₃₀H₃₃N₃O₁₃
Molecular Weight:643.604
Hs Code.:

Synonyms:nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

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Chemical Property of nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

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Technology Process of nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

There total 10 articles about nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 15862-94-9
1-(chloromethyl)-4,5-dimethoxy-2-nitrobenzene

: 185063-19-8
nitroveratryloxycarbonyl-homotyrosine methyl ester

: 185063-20-1
nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

Guidance literature:: With potassium carbonate; In acetonitrile; Heating;

Reference yield:

: 1016-58-6
6-nitroveratryl alcohol

: 185063-20-1
nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / SOCl₂ / CH₂Cl₂ / 3 h

2: 84 percent / K₂CO₃ / acetonitrile / Heating

With thionyl chloride; potassium carbonate; In dichloromethane; acetonitrile; 1: Substitution / 2: Etherification;

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 185063-20-1
nitroveratryloxycarbonyl-4-nitroveratryl-homotyrosine methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: n-BuLi / hexane; tetrahydrofuran / 3 h / -78 - 20 °C

2.1: i-Pr₂NEt / CH₂Cl₂ / 0.67 h / 0 °C

3.1: NaI / acetone

4.1: LiCl; n-BuLi; i-Pr₂NH / tetrahydrofuran; hexane / 1 h / -80 - 0 °C

4.2: 80 percent / tetrahydrofuran; hexane / 0 - 4 °C

5.1: 1 N NaOH / methanol; H₂O / 4 h / Heating

6.1: HCl(g) / 5 h / Heating

7.1: Na₂CO₃ / H₂O; dioxane / 0.5 h

8.1: 84 percent / K₂CO₃ / acetonitrile / Heating

With hydrogenchloride; sodium hydroxide; n-butyllithium; sodium carbonate; potassium carbonate; diisopropylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; lithium chloride; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; acetone; acetonitrile; 1.1: silylation / 2.1: Esterification / 3.1: Substitution / 4.1: Metallation / 4.2: Substitution / 5.1: Hydrolysis / 6.1: Esterification / 7.1: Acylation / 8.1: Etherification;