(3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

Base Information

Chemical Name:(3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine
CAS No.:1030313-79-1
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:

Synonyms:(3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

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Chemical Property of (3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

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Technology Process of (3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

There total 3 articles about (3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 13169-00-1
Methoxyallene

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 1030313-79-1
(3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

: 1030313-77-9
(3S,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

Guidance literature:: N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone; With trimethylaluminum; In hexane; dichloromethane; at 0 ℃; for 1h;

Methoxyallene; In hexane; dichloromethane; at 0 - 8 ℃; for 50h; Further stages.;
DOI:10.1002/ejoc.200700724

Reference yield: 37.0%

: 13169-00-1
Methoxyallene

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: (3R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

: 1030313-79-1
(3R,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

: 1030313-77-9
(3S,5R)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

: 1030313-78-0
(3S,5S)-2-benzyl-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-methoxy-4-methyleneisoxazolidine

Guidance literature:: N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 0.333333h;

Methoxyallene; In dichloromethane; at -78 - -65 ℃; for 1h; Further stages.;
DOI:10.1002/ejoc.200700724