Technology Process of C21H23N
There total 2 articles about C21H23N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; palladium dichloride;
In
ethanol;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol303569b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: palladium dichloride; potassium carbonate / ethanol / 0.5 h / 20 °C / Inert atmosphere
With
sodium hydride; potassium carbonate; palladium dichloride;
In
ethanol; dimethyl sulfoxide;
2.1: |Suzuki Coupling;
DOI:10.1021/ol303569b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydroxide / ethylene glycol / 4 h / Reflux; Inert atmosphere
2: cesium acetate; palladium diacetate; [bis(acetoxy)iodo]benzene; silver(I) acetate; sodium acetate / chlorobenzene; tert-butyl alcohol / 12 h / 100 °C / Inert atmosphere
With
[bis(acetoxy)iodo]benzene; silver(I) acetate; cesium acetate; sodium acetate; palladium diacetate; potassium hydroxide;
In
ethylene glycol; chlorobenzene; tert-butyl alcohol;
DOI:10.1021/ol303569b