2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

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Chemical Name:2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)
CAS No.:1164134-60-4
Molecular Formula:C₄₈H₃₂Br₄N₄NiO₄
Molecular Weight:1107.11
Hs Code.:

Synonyms:2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

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Chemical Property of 2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

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Technology Process of 2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

There total 1 articles about 2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2,3,12,13-tetrabromo-5,10,15,20-tetrakis(p-methoxyphenyl)porphyrin

: 1164134-60-4
2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

Guidance literature:: With nickel(II) acetate tetrahydrate; In N,N-dimethyl-formamide; for 2h; Reflux;
DOI:10.1021/ol901052w

Reference yield: 40.0%

: 1164134-60-4
2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

: copper(l) cyanide

: 2,3,12,13-tetracyano-meso-tetrakis(4'-methoxyphenyl)porphyrinato nickel (II)

Guidance literature:: With pyridine; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c5dt00937e

Reference yield: 24.0%

: 1164134-60-4
2,3,12,13-tetrabromo-meso-tetrakis(4'-p-tert-butylphenyl)porphyrinato nickel (II)

: 1164134-68-2
C₄₆H₃₄Br₂N₄NiO₄

Guidance literature:: With (E)-benzaldoxime sodium salt; copper(I) bromide; In dimethyl sulfoxide; at 20 - 100 ℃; for 4.25h; Inert atmosphere;
DOI:10.1021/ol901052w