methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

Base Information

Chemical Name:methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate
CAS No.:1217514-25-4
Molecular Formula:C₄₅H₄₇NO₈S
Molecular Weight:761.936
Hs Code.:

Synonyms:methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

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Chemical Property of methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

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Technology Process of methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

There total 1 articles about methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1217514-17-4
(E)-4-(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-1-(thiazol-2-yl)-but-2-en-1-one

: 167702-71-8
methyl (S)-(ethenyloxy)(phenyl)acetate

: 1217514-25-4
methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

Guidance literature:: With tris(6,6,7,7,8,8-heptafluoro-2,2-dimethyl-3,5-octadionato)europium(III); In dichloromethane; at 20 ℃; for 72h;
DOI:10.1016/j.carres.2009.11.025

Reference yield: 70.0%

: 1217514-25-4
methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

: (2R,4R)-2-[(S)-2-methyloxycarbonyl-1-phenylethoxy]-4-[(2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl]-6-formyl-3,4-dihydro-2H-pyrane

Guidance literature:: methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate; With methyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

With silver nitrate; In water; acetonitrile; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2016.09.005

Reference yield:

: 1217514-25-4
methyl (S)-2-phenyl-2-(((2R,4R)-4-((2,3,4-tri-O-benzyl-α-L-fucopyranosyl)methyl)-6-(thiazol-2-yl)-3,4-dihydro-2H-pyran-2-yl)oxy)acetate

: C₄₄H₄₇NO₇S

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2009.11.025