[La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid

Base Information

• Chemical Name: [La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid
• CAS No.: 172754-16-4
• Molecular Formula: C₆H₃N₃O₇*C₆₄H₈₆LaN₅O₁₅
• Molecular Weight: 1533.42

Synonyms:[La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid

Chemical Property of [La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid

Chemical Property:

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Technology Process of [La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid

There total 1 articles about [La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

[La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dihydroxycalix[4]arene)(picrate)3] → [La(5,11,17,23-tetra-tert-butyl-25,27-bis(diethylcarbamoylmethoxy)-26,28-dioxycalix[4]arene)(methanol)2(picrate)] * picric acid (172754-16-4)

Guidance literature:

With methanol; In methanol; dichloromethane; CH2Cl2/MeOH=1:1; crystn. on slow evapn.; elem. anal.;

DOI:10.1039/DT9950003455

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