diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

Base Information

Chemical Name:diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate
CAS No.:1170677-01-6
Molecular Formula:C₁₉H₂₉N₄O₇PS
Molecular Weight:488.502
Hs Code.:

Synonyms:diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

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Chemical Property of diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

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Technology Process of diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

There total 1 articles about diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₃N₄O₈PS

: 1170677-01-6
diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

Guidance literature:: With ammonium hydroxide; In methanol; water; at 20 ℃; for 20h;
DOI:10.1016/j.bmc.2009.04.054

Reference yield: 82.0%

: 1170677-01-6
diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate

: 1170677-05-0
{2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonic acid

Guidance literature:: diethyl {2-[N-(4-amino-1H-pyrimidin-2-on-1-ylmethyl)-N-(p-toluenesulfonyl)amino]ethoxymethyl}phosphonate; With trimethylsilyl bromide; In acetonitrile; at 20 ℃; Inert atmosphere; Cooling with ice;

With water; In acetone; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2009.04.054