[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

Base Information

Chemical Name:[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]
CAS No.:1073131-17-5
Molecular Formula:C₂₅H₂₇N₂PPdS
Molecular Weight:524.963
Hs Code.:

Synonyms:[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

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Chemical Property of [Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

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Technology Process of [Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

There total 2 articles about [Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.7%

: 1073131-16-4
[Pd(2-diphenylphosphinomethyl-2-thiazoline)(N,N-dimethylbenzylamine-C,N)](SO₃CF₃)

: 1073131-17-5
[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

Guidance literature:: With t-BuOK; In tetrahydrofuran; byproducts: KOSO2CF3; under N2; t-BuOK added to soln. of Pd complex in THF; stirred overnight; filtered; filtrate taken to dryness; extd. with toluene; extract concd. under vac.; pentane added; ppt. collected; elem. anal.;
DOI:10.1021/ic800934h

Reference yield:

: 954372-65-7
2-[(diphenylphosphino)methyl]thiazoline

: 1073131-17-5
[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: t-BuOK / tetrahydrofuran

With t-BuOK; In tetrahydrofuran;
DOI:10.1021/ic800934h

Reference yield: 93.5%

: bis[(benzyldimethylamino)chloropalladium(II)]

: 1073131-17-5
[Pd(2-diphenylphosphinomethyl-2-thiazoline(-1H))(N,N-dimethylbenzylamine-C,N)]

: 1073131-19-7
[(N,N-dimethylbenzylamine-C,N)PdCl(2-diphenylphosphinomethyl-2-thiazoline(-1H))Pd(N,N-dimethylbenzylamine-C,N)]

Guidance literature:: In tetrahydrofuran; under N2; dimeric Pd complex added to soln. Pd monomeric complex in THF;stirred overnight; concd. under reduced pressure; pentane added; ppt. washed with pentane; dried in vac.; elem. anal.;
DOI:10.1021/ic800934h