N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

Base Information

Chemical Name:N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine
CAS No.:214471-57-5
Molecular Formula:C₁₈H₂₈N₂O₆
Molecular Weight:368.43
Hs Code.:

Synonyms:N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

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Chemical Property of N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

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Technology Process of N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

There total 2 articles about N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 179688-27-8
ethyl 2-amino-4,5-bis(2-methoxyethoxy)-benzoate

: 214471-57-5
N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

Guidance literature:: ethyl 2-amino-4,5-bis(2-methoxyethoxy)-benzoate; With N,N-dimethyl-formamide; trichlorophosphate; at 0 - 55 ℃; for 1h;

With sodium hydroxide; In water; at 0 ℃;

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 179688-27-8
ethyl 2-amino-4,5-bis(2-methoxyethoxy)-benzoate

: 214471-57-5
N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

Guidance literature:: N,N-dimethyl-formamide; ethyl 2-amino-4,5-bis(2-methoxyethoxy)-benzoate; With trichlorophosphate; at 0 - 55 ℃; for 1h;

With sodium hydroxide; In dichloromethane; water; at 0 ℃; for 0.0333333h;

Reference yield:

: 214471-57-5
N'-[2-carbethoxy-4,5-bis(2-methoxyethoxy)phenyl]-N,N-dimethylformamidine

: 4-[(3-Ethynylphenyl)amino]-5,6-bis(2-methoxyethoxy)-3-quinolinecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 °C

1.2: 0.83 h

2.1: trichlorophosphate / 1.5 h / Heating / reflux

2.2: 0 °C / pH 8 - 9

3.1: pyridine hydrochloride / 2-ethoxy-ethanol / 1.5 h / Heating / reflux

With n-butyllithium; pyridine hydrochloride; trichlorophosphate; In tetrahydrofuran; 2-ethoxy-ethanol; hexane;