2-amino-5-bromobenzyltriphenylphosphonium chloride

Base Information

Chemical Name:2-amino-5-bromobenzyltriphenylphosphonium chloride
CAS No.:142906-83-0
Molecular Formula:C₂₅H₂₂BrNP*Cl
Molecular Weight:482.787
Hs Code.:

Synonyms:2-amino-5-bromobenzyltriphenylphosphonium chloride

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Chemical Property of 2-amino-5-bromobenzyltriphenylphosphonium chloride

Chemical Property:

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Technology Process of 2-amino-5-bromobenzyltriphenylphosphonium chloride

There total 3 articles about 2-amino-5-bromobenzyltriphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 142906-82-9
[(5-bromo-2-nitrophenyl)methyl]triphenylphosphonium bromide

: 142906-83-0
2-amino-5-bromobenzyltriphenylphosphonium chloride

Guidance literature:: With hydrogenchloride; zinc; In acetic acid; for 0.5h; Ambient temperature;
DOI:10.1002/jhet.5570290210

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 142906-83-0
2-amino-5-bromobenzyltriphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / conc. nitric acid, conc. sulfuric acid / 2 h / Ambient temperature

2: 100 percent / CHCl₃ / 72 h / Ambient temperature

3: 67 percent / 1.) Zn, 2.) HCl / acetic acid / 0.5 h / Ambient temperature

With hydrogenchloride; sulfuric acid; nitric acid; zinc; In chloroform; acetic acid;
DOI:10.1002/jhet.5570290210

Reference yield:

: 35287-42-4
4-bromo-2-(bromomethyl)-1-nitrobenzene

: 142906-83-0
2-amino-5-bromobenzyltriphenylphosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CHCl₃ / 72 h / Ambient temperature

2: 67 percent / 1.) Zn, 2.) HCl / acetic acid / 0.5 h / Ambient temperature

With hydrogenchloride; zinc; In chloroform; acetic acid;
DOI:10.1002/jhet.5570290210