Technology Process of C34H46Cl2N3O12P
There total 9 articles about C34H46Cl2N3O12P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid;
In
dimethyl sulfoxide;
at 37 ℃;
for 5h;
DOI:10.1021/ja411733s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride / acetonitrile / 2 h / 0 - 25 °C
2.1: 5-(ethylthio)-1H-tetrazole / acetonitrile / 2 h / 25 °C / Inert atmosphere
2.2: 0.5 h / Inert atmosphere
3.1: hydrazine / tetrahydrofuran; water / 0.08 h / 25 °C
4.1: acetic acid / dimethyl sulfoxide / 5 h / 37 °C
With
tetrabutyl ammonium fluoride; acetic acid; 5-(ethylthio)-1H-tetrazole; hydrazine;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja411733s
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: selectfluor / acetonitrile / 25 °C
2.1: tetrabutyl ammonium fluoride / acetonitrile / 2 h / 0 - 25 °C
3.1: 5-(ethylthio)-1H-tetrazole / acetonitrile / 2 h / 25 °C / Inert atmosphere
3.2: 0.5 h / Inert atmosphere
4.1: hydrazine / tetrahydrofuran; water / 0.08 h / 25 °C
5.1: acetic acid / dimethyl sulfoxide / 5 h / 37 °C
With
selectfluor; tetrabutyl ammonium fluoride; acetic acid; 5-(ethylthio)-1H-tetrazole; hydrazine;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja411733s