N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

Base Information

Chemical Name:N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine
CAS No.:181363-99-5
Molecular Formula:C₂₆H₂₅N₅O₅
Molecular Weight:487.515
Hs Code.:

N<sup>10</sup>-acetyl-N<sup>10</sup>-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N<sup>1</sup>-benzyltryptamine

Synonyms:N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

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Technology Process of N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

There total 3 articles about N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 41645-07-2
N¹-benzyl-N^ω-acetyltryptamine

: 108005-26-1
Dimethyl 3-(methylthio)-1,2,4-triazine-5,6-dicarboxylate

: 181363-99-5
N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at -30 ℃; for 0.5h;
DOI:10.1016/S0040-4020(00)00003-X

Reference yield:

: 1016-47-3
N-Acetyltryptamine

: 181363-99-5
N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / KH / tetrahydrofuran; various solvent(s) / -50 - 20 °C

2: 52 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / -30 °C

With n-butyllithium; potassium hydride; In tetrahydrofuran; hexane; 1: Alkylation / 2: Substitution;
DOI:10.1016/S0040-4020(00)00003-X

Reference yield:

: 61-54-1
tryptamine

: 181363-99-5
N¹⁰-acetyl-N¹⁰-[5,6-dicarbomethoxy-3-(1,2,4-triazinyl)]-N¹-benzyltryptamine

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / 2 h / 20 °C

2: 99 percent / KH / tetrahydrofuran; various solvent(s) / -50 - 20 °C

3: 52 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / -30 °C

With n-butyllithium; potassium hydride; triethylamine; In tetrahydrofuran; hexane; 1: Acetylation / 2: Alkylation / 3: Substitution;
DOI:10.1016/S0040-4020(00)00003-X