N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide
• CAS No.: 874894-30-1
• Molecular Formula: C₂₂H₂₁NO₄S
• Molecular Weight: 395.479

Synonyms:N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide

Chemical Property of N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide

There total 2 articles about N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-prop-2-ynyloxy-hexa-2,4-diyn-1-ol (874894-28-7) + N-allyl-N-(3-bromo-prop-2-ynyl)-4-methyl-benzenesulfonamide (874894-25-4) → N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide (874894-30-1)

Guidance literature:

With copper(l) iodide; hydroxylamine hydrochloride; N-butylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja057153c

Reference yield:

dipropargyl ether (6921-27-3) → N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide (874894-30-1)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuNH₂; aq. CuI; NH₂OH*HCl / CH₂Cl₂ / 0 - 20 °C

2: n-BuNH₂; aq. CuI; NH₂OH*HCl / CH₂Cl₂ / 0 - 20 °C

With copper(l) iodide; hydroxylamine hydrochloride; N-butylamine; In dichloromethane;

DOI:10.1021/ja057153c

Reference yield:

N-(3-bromo-prop-2-ynyl)-4-methyl-benzenesulfonamide + N-allyl-N-[6-(6-hydroxy-hexa-2,4-diynyloxy)-hexa-2,4-diynyl]-4-methyl-benzenesulfonamide (874894-30-1) → C32H30N2O5S2 (874894-32-3)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja057153c

upstream raw materials:

6-prop-2-ynyloxy-hexa-2,4-diyn-1-ol

N-allyl-N-(3-bromo-prop-2-ynyl)-4-methyl-benzenesulfonamide

dipropargyl ether

Downstream raw materials:

C₃₂H₃₀N₂O₅S₂

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