3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Base Information

Chemical Name:3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine
CAS No.:1350377-66-0
Molecular Formula:C₁₃H₂₀BNO₃
Molecular Weight:249.118
Hs Code.:
Mol file:1350377-66-0.mol

Synonyms:3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Suppliers and Price of 3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline 97%
1g
$ 675.00

Crysdot
3-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline 97%
250mg
$ 270.00

Alichem
3-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline
250mg
$ 707.00

Total 5 raw suppliers

Chemical Property of 3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

Chemical Property:

Boiling Point:387.5±32.0 °C(Predicted)
PKA:3.81±0.10(Predicted)
Density:1.08±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

3-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine

There total 3 articles about 3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)Benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 19056-40-7
4-bromo-3-methoxyaniline

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1350377-66-0
3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine; at 110 ℃; for 22h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.ejmech.2016.08.068

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 1350377-66-0
3-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / acetonitrile / 20 h / 0 - 20 °C

2: dichloro bis(acetonitrile) palladium(II); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; triethylamine / 22 h / 110 °C / Sealed tube; Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); N-Bromosuccinimide; triethylamine; In acetonitrile;
DOI:10.1016/j.ejmech.2016.08.068