C₄₇H₇₀O₉Si

Base Information

Chemical Name:C₄₇H₇₀O₉Si
CAS No.:934560-39-1
Molecular Formula:C₄₇H₇₀O₉Si
Molecular Weight:807.153
Hs Code.:

C<sub>47</sub>H<sub>70</sub>O<sub>9</sub>Si

Synonyms:C₄₇H₇₀O₉Si

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Chemical Property of C₄₇H₇₀O₉Si

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Technology Process of C₄₇H₇₀O₉Si

There total 10 articles about C₄₇H₇₀O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 934560-34-6
C₄₇H₆₉ClO₉Si

: 934560-39-1
C₄₇H₇₀O₉Si

Guidance literature:: With tri-n-butyl-tin hydride; 1,1'-azobis(1-cyanocyclohexanenitrile); In toluene; for 12h; Heating;
DOI:10.1039/b616558c

Reference yield:

: 863659-96-5
2-Methyl-2-[(2R,6S)-6-(2-oxo-ethyl)-tetrahydro-pyran-2-yl]-propionic acid methyl ester

: 934560-39-1
C₄₇H₇₀O₉Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: (+)-DIPBr / tetrahydrofuran / -78 °C

2.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

3.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

4.1: osmium tetraoxide; NMO / 12 h

4.2: 90 percent / NaIO₄ / 0.5 h

5.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

6.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

7.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

8.1: (+)-DIPBr / -78 °C

8.2: TMSCl / In(OTf)3 / CH₂Cl₂ / 4 h / 25 °C

9.1: 69 percent / ACCN; Bu₃SnH / toluene / 12 h / Heating

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; tri-n-butyl-tin hydride; sodium hydride; triethylamine; 1,1'-azobis(1-cyanocyclohexanenitrile); boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Brown allylation / 5.1: Brown crotylation / 8.1: Brown allylation / 8.2: Prins cyclization;
DOI:10.1039/b616558c

Reference yield:

: C₁₅H₂₆O₄

: 934560-39-1
C₄₇H₇₀O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

2.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

3.1: osmium tetraoxide; NMO / 12 h

3.2: 90 percent / NaIO₄ / 0.5 h

4.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

5.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

6.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

7.1: (+)-DIPBr / -78 °C

7.2: TMSCl / In(OTf)3 / CH₂Cl₂ / 4 h / 25 °C

8.1: 69 percent / ACCN; Bu₃SnH / toluene / 12 h / Heating

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; tri-n-butyl-tin hydride; sodium hydride; triethylamine; 1,1'-azobis(1-cyanocyclohexanenitrile); boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide; toluene; 4.1: Brown crotylation / 7.1: Brown allylation / 7.2: Prins cyclization;
DOI:10.1039/b616558c