7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

Base Information

Chemical Name:7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene
CAS No.:1372714-61-8
Molecular Formula:C₂₆H₃₅NO₃SSi
Molecular Weight:469.72
Hs Code.:

Synonyms:7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

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Chemical Property of 7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

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Technology Process of 7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

There total 1 articles about 7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1372714-60-7
(Z)-N-(4-((tert-butyldimethylsilyl)oxy)but-2-en-1-yl)-4-methyl-N-(3-phen-ylprop-2-yn-1-yl)benzenesulfonamide

: 1372714-61-8
7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

Guidance literature:: With platinum(IV) chloride; In 1,4-dioxane; at 25 ℃; for 1h;
DOI:10.1055/s-0031-1290314

Reference yield: 90.0%

: 1372714-61-8
7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

: 1309599-99-2
(6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-en-7-yl)methanol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 4h;
DOI:10.1055/s-0031-1290314

Reference yield:

: 1372714-61-8
7-(((tert-butyl)dimethylsilyloxy)methyl)-6-phenyl-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

: 1372714-37-8
C₂₀H₂₁NO₃S

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 25 °C

2: platinum(IV) chloride / 0.5 h / 90 °C

With tetrabutyl ammonium fluoride; platinum(IV) chloride; In tetrahydrofuran;
DOI:10.1055/s-0031-1290314