C₃₀H₃₇N₃O₄

Base Information

Chemical Name:C₃₀H₃₇N₃O₄
CAS No.:1415684-34-2
Molecular Formula:C₃₀H₃₇N₃O₄
Molecular Weight:503.641
Hs Code.:

C<sub>30</sub>H<sub>37</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:C₃₀H₃₇N₃O₄

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Chemical Property of C₃₀H₃₇N₃O₄

Chemical Property:

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Technology Process of C₃₀H₃₇N₃O₄

There total 6 articles about C₃₀H₃₇N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1415684-08-0
(10bR,12S,13R,13aS)-5,6,11,12,13,13a-hexahydro-8-methoxy-12-methyl-4H-cyclopenta[2,3]pyrrolo[2,1-a][2]benzazepine-2 (1H)-one-13-carboxylic acid

: 16015-71-7
4-(3-methoxyphenyl)piperazine

: 1415684-34-2
C₃₀H₃₇N₃O₄

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2012.10.038

Reference yield:

: 591-31-1
3-methoxy-benzaldehyde

: 1415684-34-2
C₃₀H₃₇N₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine; ammonium acetate / toluene / 71 h / Dean-Stark; Reflux

2: palladium 10% on activated carbon; hydrogenchloride; hydrogen / ethanol / 67 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

4: trifluoroacetic acid / dichloromethane / 6 h / 20 °C / Reflux

5: sodium nitrite; acetic acid / N,N-dimethyl-formamide / 7 h / 50 °C

6: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; tetrahydrofuran / 48 h / 20 °C

With pyridine; hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; ammonium acetate; hydrogen; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.tet.2012.10.038

Reference yield:

: 28446-69-7
1′-(3-methoxyphenyl)acrylonitrile

: 1415684-34-2
C₃₀H₃₇N₃O₄

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogenchloride; hydrogen / ethanol / 67 h

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

3: trifluoroacetic acid / dichloromethane / 6 h / 20 °C / Reflux

4: sodium nitrite; acetic acid / N,N-dimethyl-formamide / 7 h / 50 °C

5: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; tetrahydrofuran / 48 h / 20 °C

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.10.038