(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine

Base Information

Chemical Name:(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine
CAS No.:22195-47-7
Molecular Formula:C6H13NO2
Molecular Weight:131.175
Hs Code.:29329900
European Community (EC) Number:628-774-0
DSSTox Substance ID:DTXSID10399553
Nikkaji Number:J1.790.951G
Mol file:22195-47-7.mol

Synonyms:22195-47-7;(2,2-dimethyl-1,3-dioxolan-4-yl)methanamine;2,2-Dimethyl-1,3-dioxolane-4-methanamine;(2,2-Dimethyl-[1,3]-dioxolan-4-yl)-methylamine;2,2-Dimethyl-1,3-dioxolan-4-methylamine;1,3-Dioxolane-4-methanamine, 2,2-dimethyl-;1-(2,2-dimethyl-1,3-dioxolan-4-yl)methanamine;(2,2-Dimethyl-[1,3]-dioxolan-4-yl)methylamine;MFCD01321384;2,2-dimethyl-1,3-dioxolan-4-methanamine;SCHEMBL479143;DTXSID10399553;HXOYWCSTHVTLOW-UHFFFAOYSA-N;STR05245;GEO-01182;AKOS005257630;AB92660;AM90191;SY275114;2,2-dimethyl-4-aminomethyl-1,3-dioxolane;2.2-Dimethyl-1,3-dioxolane-4-methanamine;1,3-Dioxolane-4-methanamine,2,2-dimethyl-;CS-0080672;FT-0696016;FT-0697221;FT-0774446;(2,2-dimethyl-1,3-dioxolan-4-yl)methylamine;EN300-106876;rac-2,2-dimethyl-1,3-dioxolane-4-methanamine;(2,2-dimethyl-[1,3]dioxolan-4-yl)methyl amine;[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]amine;2,2-Dimethyl-1,3-dioxolane-4-methanamine, 97%;C-(2,2-dimethyl-[1,3]dioxolan-4-yl)-methylamine;W-200231;(S)-1-(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine;C-(2,2-Dimethyl-[1,3]dioxolan-4-yl)-methyl-amine

Suppliers and Price of (2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
2,2-Dimethyl-1,3-dioxolane-4-methanamine 97%
5g
$ 220.00

AK Scientific
2,2-Dimethyl-1,3-dioxolane-4-methanamine
5g
$ 180.00

Alichem
(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine
5g
$ 361.80

American Custom Chemicals Corporation
2,2-DIMETHYL-1,3-DIOXOLANE-4-METHANAMINE 95.00%
5G
$ 884.34

Chemenu
(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine 95%
5g
$ 308.00

Crysdot
(2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine 95+%
5g
$ 326.00

Sigma-Aldrich
2,2-Dimethyl-1,3-dioxolane-4-methanamine 97%
5g
$ 138.00

Total 42 raw suppliers

Chemical Property of (2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine

Chemical Property:

Vapor Pressure:1.59mmHg at 25°C
Refractive Index:n20/D 1.438(lit.)
Boiling Point:168.8 °C at 760 mmHg
PKA:9.16±0.29(Predicted)
Flash Point:57.6 °C
PSA：44.48000
Density:0.979 g/cm³
LogP:0.79690
XLogP3:-0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:131.094628657
Heavy Atom Count:9
Complexity:103

Purity/Quality:

98% ^*data from raw suppliers

2,2-Dimethyl-1,3-dioxolane-4-methanamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C
Statements: 34
Safety Statements: 26-27-36/37/39-45

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(OCC(O1)CN)C

Technology Process of (2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine

There total 17 articles about (2,2-Dimethyl-1,3-dioxolan-4-yl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 25261-56-7
4-(azidomethyl)-2,2?dimethyl-1,3-dioxolane

: 22195-47-7,96894-67-6
4-aminomethyl-2,2-dimethyl[1,3]dioxolane

Guidance literature:: With sodium sulfide; In methanol; at 55 ℃; for 24h;
DOI:10.1021/jo00103a054

Reference yield: 90.0%

: 40137-25-5
2-[(2,2-dimethyl-1,3-dioxolan-4-yl)methyl]-1H-isoindole-1,3(2H)-dione

: 22195-47-7,96894-67-6
4-aminomethyl-2,2-dimethyl[1,3]dioxolane

Guidance literature:: With hydrazine hydrate; In methanol; Heating;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 22195-47-7,96894-67-6
4-aminomethyl-2,2-dimethyl[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C

2: 90 percent / hydrazine monohydrate / methanol / Heating

With di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2007.05.109