1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

Base Information

Chemical Name:1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane
CAS No.:871691-68-8
Molecular Formula:C₁₄H₁₆Cl₆N₈O₄P₂S₂
Molecular Weight:699.13
Hs Code.:

Synonyms:1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

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Technology Process of 1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

There total 1 articles about 1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 57-67-0
4-amino-N-(diaminomethylene) benzenesulfonamide

: 871691-68-8
1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

Guidance literature:: With phosphorus pentachloride; In benzene; for 3h; Heating;
DOI:10.1016/j.saa.2004.12.047

Reference yield: 76.0%

: 871691-68-8
1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

: copper(II) choride dihydrate

: 7732-18-5
water

: [(CuCl)2(1,3-[N'-amidino-sulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane(-2H))(H₂O)6]

Guidance literature:: In ethanol; byproducts: HCl; soln. of Cu salt (2 equiv.) in dry ethanol was added dropwise with stirring to soln. of ligand (1 equiv.) in abs. ethanol at room temp.; mixt. was refluxed for 2 h under dry conditions; washed with dry ethanol and dry Et2O; dried (vac.); elem. anal.;
DOI:10.1016/j.saa.2004.12.047

Reference yield: 65.0%

: 871691-68-8
1,3-di-[N'-amidinosulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane

: cadmium(II) chloride monohydrate

: 7732-18-5
water

: [(CdCl)(1,3-[N'-amidino-sulfanilamide]-2,2,2,4,4,4-hexachlorocyclodiphosph(V)azane(-2H))(H₂O)6]

Guidance literature:: In ethanol; byproducts: HCl; soln. of Cd salt (2 equiv.) in dry ethanol was added dropwise with stirring to soln. of ligand (1 equiv.) in abs. ethanol at room temp.; mixt. was refluxed for 2 h under dry conditions; washed with dry ethanol and dry Et2O; dried (vac.); elem. anal.;
DOI:10.1016/j.saa.2004.12.047