[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Base Information

Chemical Name:[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline
CAS No.:1440912-64-0
Molecular Formula:C₂₁H₂₆FNO₃
Molecular Weight:360.43
Hs Code.:

[<sup>13</sup>C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Synonyms:[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Chemical Property:

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Technology Process of [¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

There total 7 articles about [¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1440912-82-2
[¹³C]-4-methylaminobenzaldehyde

: 1440912-53-7
diethyl 4-(2-(2-(2-Fluoroethoxy)ethoxy)ethoxy)-benzylphosphonate

: 1440912-64-0
[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Guidance literature:: With sodium ethanolate; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1021/jo400741t

Reference yield:

: 101455-14-5
2-(2-(2-(p-tolyloxy)ethoxy)ethoxy)ethan-1-ol

: 1440912-64-0
[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; dmap / dichloromethane / 1.5 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / Microwave irradiation; Heating

3: N-Bromosuccinimide; Perbenzoic acid / tetrachloromethane / 4 h / Reflux

4: zinc dibromide / dichloromethane / 18 h / 20 °C

5: sodium ethanolate / N,N-dimethyl-formamide / 60 °C

With dmap; N-Bromosuccinimide; Perbenzoic acid; tetrabutyl ammonium fluoride; sodium ethanolate; triethylamine; zinc dibromide; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo400741t

Reference yield:

: 1304773-45-2
1-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)-4-methylbenzene

: 1440912-64-0
[¹³C]-(E)-4-(4-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)styryl)-N-methylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; Perbenzoic acid / tetrachloromethane / 4 h / Reflux

2: zinc dibromide / dichloromethane / 18 h / 20 °C

3: sodium ethanolate / N,N-dimethyl-formamide / 60 °C

With N-Bromosuccinimide; Perbenzoic acid; sodium ethanolate; zinc dibromide; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo400741t