4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N

Base Information

• Chemical Name: 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N
• CAS No.: 1131217-93-0
• Molecular Formula: C₂F₆NO₄S₂*C₂₉H₂₅F₆N₂S
• Molecular Weight: 827.736

Synonyms:4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N

Chemical Property of 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N

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Technology Process of 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N

There total 2 articles about 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

5-iodo-1,3,4-trimethyl-2-phenyl-1H-imidazolium bis(trifluoromethanesulfonyl)imide (1131218-20-6) + 2-(2,3,3,4,4,5,5-heptefluorocyclopent-1-en-1-yl)-2,4-dimethyl-5-phenylthiophene (362513-29-9) → 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf2N (1131217-93-0)

Guidance literature:

5-iodo-1,3,4-trimethyl-2-phenyl-1H-imidazolium bis(trifluoromethanesulfonyl)imide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

2-(2,3,3,4,4,5,5-heptefluorocyclopent-1-en-1-yl)-2,4-dimethyl-5-phenylthiophene; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;

DOI:10.1002/chem.200801192

Reference yield:

C2F6NO4S2(1-)*C29H25F6N2S(1+) → 4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf2N (1131217-93-0)

Guidance literature:

Vis irradiation;

DOI:10.1002/chem.200801192

Reference yield:

4-(2-(2,4-dimethyl-5-phenylthiophene-3-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-enyl)-1,3,5-trimethyl-2-phenyl-1H-imidazolium Tf2N (1131217-93-0) → C2F6NO4S2(1-)*C29H25F6N2S(1+)

Guidance literature:

In 2-methyltetrahydrofuran; UV-irradiation;

DOI:10.1002/chem.200801192

upstream raw materials:

5-iodo-1,3,4-trimethyl-2-phenyl-1H-imidazolium bis(trifluoromethanesulfonyl)imide

2-(2,3,3,4,4,5,5-heptefluorocyclopent-1-en-1-yl)-2,4-dimethyl-5-phenylthiophene

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