2,6-dimethoxyphenyl chlorothionocarbonate

Base Information

• Chemical Name: 2,6-dimethoxyphenyl chlorothionocarbonate
• CAS No.: 128292-47-7
• Molecular Formula: C₉H₉ClO₃S
• Molecular Weight: 232.688
• Mol file: 128292-47-7.mol

Synonyms:2,6-dimethoxyphenyl chlorothionocarbonate

Chemical Property of 2,6-dimethoxyphenyl chlorothionocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2,6-dimethoxyphenyl chlorothionocarbonate

There total 1 articles about 2,6-dimethoxyphenyl chlorothionocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

thiophosgene (463-71-8) + sodium salt of 2,6-dimethoxyphenol (71912-90-8) → 2,6-dimethoxyphenyl chlorothionocarbonate (128292-47-7)

Guidance literature:

In tetrahydrofuran; at 0 ℃;

Reference yield: 88.0%

2,6-dimethoxyphenyl chlorothionocarbonate (128292-47-7) + (3S,8S,9S,10R,13S,14S,16R,17R)-17-((1S,2R)-2-Hydroxy-1,5-dimethyl-hexyl)-10,13-dimethyl-3-(tetrahydro-pyran-2-yloxy)-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-16-ol (128292-38-6) → C41H62O7S (128292-46-6)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 ℃; for 72h;

Reference yield:

2,6-dimethoxyphenyl chlorothionocarbonate (128292-47-7) → C44H70O7SSi (128322-43-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / pyridine, DMAP / CH₂Cl₂ / 72 h / 0 °C

2: 90 percent / pyridine

With pyridine; dmap; In dichloromethane;

upstream raw materials:

thiophosgene

sodium salt of 2,6-dimethoxyphenol

Downstream raw materials:

C₄₁H₆₂O₇S

C₄₄H₇₀O₇SSi