10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

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Chemical Name:10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester
CAS No.:1634721-93-9
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

Synonyms:10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

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Chemical Property of 10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

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Technology Process of 10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

There total 5 articles about 10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1634721-99-5
4-(2-ethoxycarbonylethyl)-3-oxo-2-phenyl-3,4-dihydro-2H-quinoxaline-1-carboxylic acid benzyl ester

: 1634721-93-9
10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 10 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.14233/ajchem.2014.15859

Reference yield:

: 1634722-04-5
3-oxo-2-phenyl-3,4-dihydro-2H-quinoxalin-1-carboxylic acid benzyl ester

: 1634721-93-9
10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.14233/ajchem.2014.15859

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1634721-93-9
10-phenyl-3,4,10,10a-tetrahydro-2H-1-oxa-4a,9-diazaphenanthrene-9-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 5 h / 60 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 12 h / 80 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.14233/ajchem.2014.15859