benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

Base Information

Chemical Name:benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate
CAS No.:1242104-12-6
Molecular Formula:C₃₇H₄₈N₂O₇Si
Molecular Weight:660.883
Hs Code.:

Synonyms:benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

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Chemical Property of benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

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Technology Process of benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

There total 1 articles about benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1242104-11-5
C₃₇H₄₆N₂O₇Si

: 1242104-12-6
benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2S,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

: benzyl (S)-1-(4-(tert-butyldiphenylsilyloxy)butylamino)-3-((1R,2R,4R,5S)-2,5-dihydroxy-7-oxabicyclo[2.2.1]heptan-2-yl)-1-oxopropan-2-ylcarbamate

Guidance literature:: With cyclohexa-1,4-diene; bis(cyclopentadienyl)titanium chloride; In tetrahydrofuran; at 0 ℃; for 6h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol1017189