6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

Base Information

Chemical Name:6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide
CAS No.:1428336-00-8
Molecular Formula:C₃₆H₃₂N₆O₄
Molecular Weight:612.688
Hs Code.:

Synonyms:6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

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Chemical Property of 6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

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Technology Process of 6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

There total 6 articles about 6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1428336-01-9
N-(4-methoxybenzyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine

: 1428335-99-2
6-bromo-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)picolinamide

: 1428336-00-8
6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In water; acetonitrile; at 80 - 100 ℃; for 2h; Sealed tube; Inert atmosphere;

Reference yield:

: 1428335-97-0
2-morpholino-6-nitro-5-phenylbenzo[d]oxazole

: 1428336-00-8
6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: iron; hydrogenchloride / ethanol; water / 2 h / 70 - 80 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 - 30 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; acetonitrile / 2 h / 80 - 100 °C / Sealed tube; Inert atmosphere

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; iron; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1428335-98-1
C₁₇H₁₇N₃O₂

: 1428336-00-8
6’-((4-methoxybenzyl)amino)-N-(2-morpholino-5-phenylbenzo[d]oxazol-6-yl)-[2,3'-bipyridine]-6-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 24 h / 20 - 30 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; acetonitrile / 2 h / 80 - 100 °C / Sealed tube; Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In water; N,N-dimethyl-formamide; acetonitrile;